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BS ISO 4942:2016

$102.76

Steels and irons. Determination of vanadium content. N-BPHA spectrophotometric method

Published By Publication Date Number of Pages
BSI 2016 20
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This document specifies an N-benzoylphenylhydroxylamine (N-BPHA) spectrophotometric method for the determination of vanadium in steels and cast irons.

This document is applicable to vanadium contents between 0 ,005 % and 0,50 % (mass fraction).

PDF Catalog

PDF Pages PDF Title
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
9 6 Apparatus
7 Sampling
8 Procedure
8.1 Test portion
8.2 Blank test
10 8.3 Determination
8.3.1 Preparation of the test solution
8.3.2 Oxidation of vanadium
8.3.3 Colour development and extraction
8.3.4 Spectrophotometric measurements
11 8.4 Establishment of the calibration curve
8.4.1 Preparation of the calibration solutions
8.4.2 Spectrophotometric measurements
8.4.3 Plotting of the calibration curve
9 Expression of results
9.1 Method of calculation
12 9.2 Precision
13 10 Special cases
11 Test report
14 Annex A (informative) Additional information on the international interlaboratory test
15 Annex B (informative) Graphical representation of precision data
16 Bibliography
BS ISO 4942:2016
$102.76