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BS ISO 13909-7:2016

$198.66

Hard coal and coke. Mechanical sampling – Methods for determining the precision of sampling, sample preparation and testing

Published By Publication Date Number of Pages
BSI 2016 54
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PDF Catalog

PDF Pages PDF Title
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
4 General
10 5 Formulae relating to factors affecting precision
5.1 General
11 5.2 Sampling
12 6 Estimation of primary increment variance
6.1 Direct determination of individual primary increments
13 6.2 Determination using the estimate of precision
7 Methods for estimating precision
7.1 General
7.2 Duplicate sampling with twice the number of increments
16 7.3 Duplicate sampling during routine sampling
17 7.4 Alternatives to duplicate sampling
7.5 Precision adjustment procedure
18 8 Calculation of precision
8.1 Replicate sampling
19 8.2 Normal sampling scheme
20 9 Methods of checking sample preparation and testing errors
9.1 General
9.2 Target value for variance of sample preparation and analysis
9.2.1 General
21 9.2.2 Off-line preparation
9.2.3 On-line preparation
9.3 Checking procedure as a whole
22 9.4 Checking stages separately
9.4.1 General
23 9.4.2 Procedure 1
26 9.4.3 Procedure 2
29 9.4.4 Interpretation of results
30 9.5 Procedure for obtaining two samples at each stage
9.5.1 With a riffle
9.5.2 With a mechanical sample divider
9.6 Example
34 Annex A (informative) Variogram method for determining variance
42 Annex B (informative) Grubbs’ estimators method for determining sampling precision
51 Bibliography
BS ISO 13909-7:2016
$198.66