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BS EN ISO 4945:2018

$102.76

Steel. Determination of nitrogen. Spectrophotometric method

Published By Publication Date Number of Pages
BSI 2018 22
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This document specifies a spectrophotometric method for the determination of nitrogen in steel.

The method is applicable to the determination of nitrogen mass fraction between 0,000 6 % and 0,050 % in low alloy steels and between 0,010 % and 0,050 % in high alloy steels.

The method does not apply to samples containing silicon nitrides or having silicon contents higher than 0,6 %.

PDF Catalog

PDF Pages PDF Title
2 National foreword
4 European foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
8 5 Reagents
9 6 Apparatus
7 Sampling
8 Procedure
8.1 Test portion
10 8.2 Blank test
8.3 Determination
8.3.1 Dissolution
8.3.2 Treatment of insoluble residue
8.3.3 Steam distillation (see Figure A.1, A.2 or A.3)
11 8.3.4 Formation of the coloured complex
8.3.5 Spectrophotometric measurements
8.4 Establishment of the calibration curve
8.4.1 Preparation of the calibration solutions
12 8.4.2 Spectrophotometric measurements
8.4.3 Plotting the calibration curve
9 Expression of results
9.1 Method of calculation
13 9.2 Precision
10 Test report
14 Annex A (informative) Examples of distillation apparatus
17 Annex B (informative) Additional information on the international interlaboratory test
20 Annex C (informative) Graphical representation of precision data
21 Bibliography
BS EN ISO 4945:2018
$102.76