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BS EN 17251:2020

BS EN 17251:2020

$102.76

Foodstuffs. Determination of ochratoxin A in pork meat and derived products by IAC clean-up and HPLC-FLD

Published By Publication Date Number of Pages
BSI 2020 22
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This document describes a procedure for the determination of ochratoxin A (OTA) in pork products specifically ham, pork-based products (canned chopped pork) and pork liver using high performance liquid chromatography with fluorescence detection (HPLC-FLD).

The method has been validated for ochratoxin A in naturally contaminated ham, pork based products (canned chopped pork) and pork liver containing 0,5 ?g/kg to 11 ?g/kg [4], [5], [6].

Laboratory experiences have shown that this method is also applicable to pĆ¢tĆ© and kidney [4].

PDF Catalog

PDF Pages PDF Title
2 undefined
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
10 6 Apparatus and equipment
11 7 Procedure
7.1 Preparation of the test sample
7.2 Extraction of ochratoxin A
7.2.1 General
12 7.2.2 Immunoaffinity column clean-up
7.3 Spiking procedure
8 HPLC-FLD analysis
8.1 General
13 8.2 HPLC operating conditions
8.3 Calibration curve
8.4 Identification
9 Calculation
14 10 Precision
10.1 General
10.2 Repeatability
10.3 Reproducibility
15 11 Test report
16 Annex A (informative)Typical chromatograms
19 Annex B (informative)Precision data

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BS EN 17251:2020
$102.76