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ASTM-E2253 2011

$40.63

E2253-11 Standard Test Method for Temperature and Enthalpy Measurement Validation of Differential Scanning Calorimeters

Published By Publication Date Number of Pages
ASTM 2011 7
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1.1 This test method provides procedures for validating temperature and enthalpy measurements of differential scanning calorimeters (DSC) and analytical methods based upon the measurement of temperature or enthalpy (or heat), or both, by DSC. Performance parameters determined include temperature and calorimetric repeatability (precision), detection limit, quantitation limit, linearity, and bias. This test method is applicable to exothermic events.

1.2 Validation of apparatus performance and analytical methods is requested or required for quality initiatives or where results may be used for legal purposes.

1.3 The values stated in SI units are to regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of Test Method
2 Significance and Use
Apparatus
Reagents and Materials
Calibration and Standardization
Procedure for Determining Calorimetric Repeatability, Detection Limit, Quantitation Limit, Linearity, and Bias
3 FIG. 1
4 Procedure for Determining Temperature Repeatability, Detection Limit, Quantification Limit, Linearity, and Bias
FIG. 2
TABLE 1
5 FIG. 3
6 Calculations
Example Calculations
7 Report
Precision and Bias
Keywords
ASTM-E2253 2011
$40.63